| 1 |
0 |
7k |
| answers |
votes |
views |
Hi, I am unable to activate our lift on our avance III 400 NMR from BruKer The message is emergency air lift activated....
| 4 |
0 |
5k |
| answers |
votes |
views |
Hi.We have a 500MHz BRUKER AVANCE spectrometer.unfortunately its has been quenched.we have 3 probes:5mmQNP , 5mmBBI and ...
| 0 |
0 |
1k |
| answers |
votes |
views |
Hi. I receive this error, when I try to modify the wiki.
Fatal error: Cannot redeclare class MWNamespace in /var/www/nm...
| 0 |
0 |
1k |
| answers |
votes |
views |
I upload my protein on csrosetta server for generating structures. I have provided TALOS data file.
Its already two days...
Posted:
anup
1
Jun 04 '13 at 06:09
| 1 |
0 |
3k |
| answers |
votes |
views |
I was running a 3D 15N edit NOESY (on a Bruker 600) and it was inadvertently stopped. I would like to restart the experi...
| 0 |
0 |
2k |
| answers |
votes |
views |
Hello,
I have some users interested in measuring a ROESY build-up curve for their samples (NOESY does not work due to m...
Posted:
sararah
11
Jun 10 '13 at 08:30
| 0 |
0 |
2k |
| answers |
votes |
views |
Hi, thank you for reading my question. I am a novice at NMR, I apologize in advance if my question appears naive. I am ...
Posted:
pjb
1
Jun 11 '13 at 00:32
| 2 |
0 |
6k |
| answers |
votes |
views |
Hey everyone,
I've started practicing reading NMR again after having not done so for years, and I'm getting caught up o...
| 0 |
0 |
2k |
| answers |
votes |
views |
Hi,
I need to run FMR (ferromagnetic resonance) on Bruker x-band CW EPR spectrometer. I know it can be done, but I would...
Posted:
nmrman
1
Jun 14 '13 at 07:52
| 1 |
0 |
3k |
| answers |
votes |
views |
Dear everyone,
I was wondering how can I know the number of unambiguous noe assignments both after manual assignment an...
Posted:
Yar
13
/ Updated:
eiso
31
Jul 10 '13 at 04:24
| 0 |
0 |
2k |
| answers |
votes |
views |
Hello
I am using satxfer1D experiment on varian unity plus 500 MHz spectrometer and vnmr (not vnmrJ!) software. I would...
Posted:
Kate
1
Jun 26 '13 at 04:59
| 0 |
0 |
5k |
| answers |
votes |
views |
HELLO all nmr wikier,
I am facing problem in hsqc experiment on bruker machine using pulse prog hsqcetgpsi
Normally the ...
Posted:
feroon
21
Jun 27 '13 at 10:09
| 3 |
0 |
6k |
| answers |
votes |
views |
Hi, I am new here!
I am working on Bruker 600 MHz over 10 years, but now I have problem to get 35Cl NMR spectrum.
I use...
| 2 |
0 |
4k |
| answers |
votes |
views |
Hy everyone,
I'm having a strange problem when reading the NMR spectrum of a small aromatic molecule in deuterium oxide:...
Updated:
Ruggero
3
Jul 15 '13 at 03:22
| 2 |
0 |
3k |
| answers |
votes |
views |
I had a very weird situation where my compound shows double bond between carbons in NMR but shows it as single bond in x...
| 2 |
0 |
3k |
| answers |
votes |
views |
Hello all,
I am working with a varian spectrometer and did a 2D experiment with a 3D pulse sequence and I need help with...
Updated:
PBjang
1
Jul 17 '13 at 01:39
| 1 |
0 |
13019 |
| answers |
votes |
views |
Dear Colleagues:
I've varian nmr 300, and i've a problem with the spinner that doesn't eject, it stucked like it is froz...
| 1 |
0 |
3k |
| answers |
votes |
views |
Hi all,
I have a 2D Bruker dataset that took a while to acquire, so I'd rather not simply repeat it. However, it seems...
| 2 |
0 |
3k |
| answers |
votes |
views |
Hello All
Does anyone have any ideas on why the S/N would increase and then degrade during an HMBC-style experiment? I...
| 2 |
0 |
3k |
| answers |
votes |
views |
Can someone please help me solve an nmr problem? I've tried a lot but can't get it. Please post ur email and i'll send y...
| 1 |
0 |
4k |
| answers |
votes |
views |
I have run a 1H-103Rh HMQC on [Rh(acac)(cod)] and found the chemical shift of the 103Rh to be -7023 ppm. The frequency ...
| 2 |
0 |
6k |
| answers |
votes |
views |
how do we decide on power levels and lengths of purge gradients in a new experiment?...As for coherence selection, relat...
Updated:
nmr2rmn
3
Aug 09 '13 at 14:58
| 2 |
0 |
5k |
| answers |
votes |
views |
Hi everyone,
Has someone tried to run proton decoupled of 14N? How long should be the 14N decoupling pulse? I had some ...
| 0 |
0 |
2k |
| answers |
votes |
views |
Hi,
I am using gaussian 09 to simulate proton NMR and I am comparing my results with the ones published here:
Atieh, Z...
Posted:
LFF
1
Aug 16 '13 at 04:09
| 2 |
0 |
4k |
| answers |
votes |
views |
Hi all,
i'd like to hear some experiences you folks had on this theme.
I wanna by a program for that. Just googling for...
Posted:
fid
139
/ Updated:
ehaapani
1
Oct 07 '13 at 01:11
| 2 |
0 |
5k |
| answers |
votes |
views |
I use a Bruker Avance 400 III, when using topshim command the following error appear: 'wait for event-acquisition runnin...
| 2 |
0 |
10442 |
| answers |
votes |
views |
Hi,
I am trying to collect 1D NOESY spectrum of a small protein in 90% H2O with selective excitation so I could follow ...
| 0 |
0 |
2k |
| answers |
votes |
views |
Hi !
I need a macro that can determine the standard deviation of the spectral noise for a many
similar 2D spectra.
I h...
| 4 |
0 |
21816 |
| answers |
votes |
views |
We have got a donated AQR/p with Spectrospin 300 magnet and there is no helium inside. It was sitting in the warehouse f...
| 2 |
0 |
5k |
| answers |
votes |
views |
Hi all,
I need to make a figure containing a 2D NMR spectrum for a paper. Has anyone figured out a good way to do this...
| 3 |
0 |
8k |
| answers |
votes |
views |
Is it possible to run a 13C spectra in which one carbon is coupled (with 1H) and remaining carbons are decoupled, using ...
| 1 |
0 |
2k |
| answers |
votes |
views |
hello everyone
I have a problem in opening vnmr file into sparky.
i have converted vnmr file into ucsf, when this file ...
| 2 |
0 |
5k |
| answers |
votes |
views |
Hello,
I have a DOSY data set in TopSpin and I'd like to extract diffusion coefficients for two small peaks in the spec...
| 2 |
0 |
5k |
| answers |
votes |
views |
how T1 and T2 relaxation time depend on nmr signal?
...
| 2 |
0 |
4k |
| answers |
votes |
views |
Hi!
I need to know how to reference nitrogen 15 from proton in a foldel hsqc experiment...I don't know how to calculate ...
| 1 |
0 |
2k |
| answers |
votes |
views |
I known how to pick peaks automatically. But it always omits some small peaks and picks some noise as peaks. Is there an...
| 2 |
0 |
33237 |
| answers |
votes |
views |
Hi All,
I've been trying to get a clear answer to this question for a while now, but can't seem to get a definitive ...
| 5 |
0 |
3k |
| answers |
votes |
views |
Hi,
We have a Bruker MAS probe (4mm, late 90s vintage, widebore) that reports a spin speed twice what it is actually doi...
| 1 |
0 |
7k |
| answers |
votes |
views |
I have prepared a sealed DMSO-d6 capillary tube (3mmOD) to use as an internal reference for an undergraduate prac using ...
| 2 |
0 |
7k |
| answers |
votes |
views |
Hello All
Does anyone have any ideas on what might give a phosphorus signal at negative 74 ppm (cf phosphoric acid)? T...
Updated:
Craig
41
Nov 19 '13 at 05:11
| 1 |
0 |
3k |
| answers |
votes |
views |
Are there any problems with doing proton NMR of a compound containing iron?
...
Updated:
Debbie
1
Nov 15 '13 at 10:43
| 0 |
0 |
3k |
| answers |
votes |
views |
Hi,
I do not know how to convert a data set acquired using Spinsight into a format that can be read by Topspin. The d...
Posted:
mike
1
Nov 14 '13 at 14:00
| 1 |
0 |
2k |
| answers |
votes |
views |
Hi, I am new in NMR. Can someone please answer me why prefer N-NMR but not C and H -NMR?
Thanks
...
| 4 |
0 |
8k |
| answers |
votes |
views |
hi All,
I run a 1H-15N HMBC experiment on a Bruker AVANCE III 600 MHz spectrometer. But I fail to get the long- range ...
| 2 |
0 |
8k |
| answers |
votes |
views |
Hello all,
I have used stretched polyacrylamide gels successfully many times to collect RDC data for proteins. The las...
Updated:
ChemMJW
99
Dec 06 '13 at 19:10
| 2 |
0 |
5k |
| answers |
votes |
views |
I have some older 2D HSQC 1H-15N data that was run by a NMR tech. Is there a way I can tell what kind of solvent suppre...
| 0 |
0 |
1k |
| answers |
votes |
views |
One can roughly set the integral start and end by left clicking in the spectra. Is there a command which let you type in...
Posted:
de xiao
11
Nov 27 '13 at 07:58
| 0 |
0 |
1k |
| answers |
votes |
views |
Dear all!
I am struggling with some density matrices in PHIP experiments.
I understand why the density matrix before hyd...
| 1 |
0 |
3k |
| answers |
votes |
views |
In the decoupled HSQC of a polypetide I see two small peaks right and left to the delta arginine signal. These peaks hav...
| 2 |
0 |
5k |
| answers |
votes |
views |
I recently read an article about executing a WET sequence for water suppression in urine samples. The 90°excitation puls...
