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Hi All,
I am worikng with 500Mhz Bruker. Recently 3rd channel is installed in my institute when i run 3D HNCA experime...
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Hi, comrades! We use the linux version of TopSpin 2.1 as a software for AVANCE II Bruker 400 MHz.
As I found parameters ...
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I would like to know what is the command being used to read the parameter files of bruker when 'Read Parameter' button i...
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Hi i'm a newbie in NMR and I have 2 proteins, A protein is about 12KDa, B protein is about 45 KDa,i know that A protein ...
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10667 |
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I had just finished refilling the nitrogen and powering up the NMR after the holiday shutdown and went through the norma...
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I want to get second moment from fid data. Does anyone know how to do it or is there any free computer program solving s...
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Is is an average k? And how could we extract the k of forward and backward reaction?
...
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Could anyone tell the reason why adenine h2 has a longer T1 and T2 than the other prontons in nucleic acid? It would be ...
Updated:
yuan
1
Jan 13 '13 at 22:36
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7k |
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I have a question regarding the quantification of the error in peak integrals due to noise.
I have a series of spectra ...
1 |
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Ok, let's face it. I don't know what I'm doing. I'm a separations chemist running our NMR. sigh.
Anyway, I have been co...
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Hi,
I recently run 195Pt-1H HMBC from one platinum compound with phosphorous and methyl group, unfortunately the counte...
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15199 |
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Dear all,
I am new to NMR and I have difficulty understanding the ordering of FIDs, e.g. if an experiment uses both Ran...
Updated:
nmr2rmn
3
Mar 27 '13 at 02:12
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Hello all,
Our daily check sample for the Minispec mq40 has been decreased in volume due to probably evaporation!!
An...
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5k |
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I am working with carbohydrates and in 1D NMR we have anomeric protons very close to the HOD peak, sometimes even right ...
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Hi,
I have been trying to implement some pulse sequences from literature into Bruker format. However, when it comes to t...
Posted:
nmrman
1
/ Updated:
Jana
31
Apr 14 '13 at 21:11
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Hi.we have a 500MHz AVANCE-bruker but unfortunatly it's has been quenched.our konsole has been off for about 6 month and...
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Hii,
I want to know the difference between 13C edited and 13C resolved NOESY and also tell me about the applicati...
1 |
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How to set up the experiment in order to obtain a good COSY spectrum of Cu(II) compound?
I have tried to do it by just ...
1 |
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8k |
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Hi, I am unable to activate our lift on our avance III 400 NMR from BruKer The message is emergency air lift activated....
1 |
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I was running a 3D 15N edit NOESY (on a Bruker 600) and it was inadvertently stopped. I would like to restart the experi...
1 |
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Dear everyone,
I was wondering how can I know the number of unambiguous noe assignments both after manual assignment an...
Posted:
Yar
13
/ Updated:
eiso
31
Jul 10 '13 at 04:24
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13419 |
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Dear Colleagues:
I've varian nmr 300, and i've a problem with the spinner that doesn't eject, it stucked like it is froz...
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Hi all,
I have a 2D Bruker dataset that took a while to acquire, so I'd rather not simply repeat it. However, it seems...
1 |
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I have run a 1H-103Rh HMQC on [Rh(acac)(cod)] and found the chemical shift of the 103Rh to be -7023 ppm. The frequency ...
1 |
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6k |
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What do we exactly mean by "utilizing steady state polarization" to gain sensitivity in an experiment?...I know that ste...
Updated:
nmr2rmn
3
Aug 07 '13 at 14:05
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72442 |
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Hi all, I have a small question on how to aquired a complete signal in BRUKER AVIII.
I want to create a multi pulse sequ...
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hello everyone
I have a problem in opening vnmr file into sparky.
i have converted vnmr file into ucsf, when this file ...
1 |
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I known how to pick peaks automatically. But it always omits some small peaks and picks some noise as peaks. Is there an...
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8k |
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I have prepared a sealed DMSO-d6 capillary tube (3mmOD) to use as an internal reference for an undergraduate prac using ...
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Are there any problems with doing proton NMR of a compound containing iron?
...
Updated:
Debbie
1
Nov 15 '13 at 10:43