Tagged questions

How to adjust the receiver gain in a deuterium oxide protein sample?

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I am running a 15N HSQC on a protein sample which is in a 100% deuterium oxide solvent. The command rga in TopSpin gives...
Updated: norsouth 3 Dec 02 '13 at 11:16

Setting up deuterium (2H) NMR on Bruker BBO probe

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I need to set up 2H NMR on a Bruker 600 MHz BBO probe for the first time. Can anyone give me a set of instructions? Do ...
Posted: doodlebugs 1 / Updated: Anne Baudouin 36 Oct 15 '12 at 02:37

SSNMR 2H wideline probe that can access sample temperatures in the range of 20-150 K?

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Is anyone aware of NMR facilites, which possess a SSNMR equipped with a 2H wideline probe that can access sample tempera...
Posted: Cortnie Vogelsberg 21 / Updated: Alexey Potapov 21 Jul 04 '11 at 10:24

Should I decouple deuterium on 2H/15N labeled sample for R1, R2 and hetnoe?

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If I'm running relaxation experiments (15N) for R1, R2, and hetnoe on a double labeled (2H/15N) sample, do I need to do ...
Posted: anita 31 / Updated: roseyp 46 Sep 01 '10 at 12:55

What has been done with direct detection of Deuterium?

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Hello, I am trying to investigate what has been done in NMR using direct detection of deuterium in liquids. - Could you ...
Updated: Evgeny Fadeev 5771 Jul 25 '10 at 14:49

How to best correlate Deuterium with other nuclei by NMR?

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Hello, I've been asked to solve a problem of assigning a positon of deuteration on a molecule, where structure of the de...
Posted: Evgeny Fadeev 5771 / Updated: kiscs kiscs 21 May 17 '10 at 16:43
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