How to confirm structure of propane by NMR?

2 2 5k
answers votes views
I will really need your help. I am chemist working in the oil buisness and I am interesting is it possible to analyze pr...
ron daedalus 11 Apr 21 '10 at 09:18

Using probe that started losing B1 strength or has longer 90 degree pulse

1 0 5k
answers votes views
I've found that one of our probes lost ~1.5-2 dB of power on 13C, but nutation curve looks OK. There are no random spike...
Joseph DiVerdi 146 Apr 19 '10 at 18:07

How to explain binary-like pattern in the nutation curve in a simple 90 degree pulse calibration experiment?

1 0 8k
answers votes views
Hello, I wanted to ask this in a while. Finally a sample arrived that shows this behavior and I made a screenshot (below...
Joseph DiVerdi 146 Apr 15 '10 at 17:23

How to optimally choose a 1/4J 1H-15N delay for INEPT?

2 1 7k
answers votes views
Why is it often the case that when transferring magnetization from 1H to 15N, the 1/4J time is often a little less than ...
Evgeny Fadeev 5771 Apr 14 '10 at 16:33

How to set up EPR measurement at elevated temperatures?

0 0 3k
answers votes views
What setup do you use to measure EPR at temperatures above room temperature? We have a Bruker EMX500 instrument and we...
Evgeny Fadeev 5771 Apr 14 '10 at 16:28

Why are my acetic acid-d4 solvent peaks off from the expected ppm value?

1 1 8k
answers votes views
Hello there. After running an 1H-NMR experiment I observed the acetic acid-d4 solvent peaks at 11.54 and 21.16 ppm (off...
Evgeny Fadeev 5771 Apr 12 '10 at 15:08

Reduced dimensionality experiments in BioPack

1 1 6k
answers votes views
could anyone suggest pulse sequences that are available in Varian's BioPack that can be readily run in reduced-dimension...
David Leonen 1 Apr 11 '10 at 22:26

How do you calculate the % or degree of acrylation of a polymer using integrated NMR peaks?

2 1 20461
answers votes views
Hello, I'm trying to use an NMR spectrum to define/calculate a "degree of acrylation" for a PLA-PEG-PLA block copolymer ...
juxtabo 11 Apr 11 '10 at 10:48

In ModelFree calculations how to deal with spins not assigned to models and vice versa?

0 1 5k
answers votes views
What does it mean when modelfree does not assign any model to a particular spin? Also, what should one do if more than h...
Evgeny Fadeev 5771 Apr 07 '10 at 09:13

What is the definition of term Saturation and what are ways to achieve that state?

2 1 20896
answers votes views
Hello. What is the best definition to the state of "saturation" in the context of NMR? No phase coherence in the transv...
Joseph DiVerdi 146 Apr 06 '10 at 20:44
680

questions

Questions are sorted by the time of last update. Most recently answered questions are shown first.

Tags

× 34
× 25
× 11
× 10
× 10
× 10
× 9
× 8
× 6
× 5
× 5
× 5
× 4
× 4
× 4
× 3
× 3
× 3
× 2
× 2
× 1
× 1
× 1
× 1
× 1
posts per page103050

powered by CNPROG