Unanswered questions

1H-31P Hetcore with Varian inova 500, How can it be possible?

4 2 8k
answers votes views
I use a varian inova 500 NMR machine. it has vnmrj 2.1B software. An auto-x pfg 500 Mhz probe and auto tuning unit also....
Ulrich Haunz 210 Apr 27 '10 at 00:34

How to assign (perturbed) resonances when structure is known?

1 0 5k
answers votes views
I had two problems like this one recently: have protein (in solution) of known general structure resonance assignments...
Aleksandr Yakimov 11 Apr 25 '10 at 01:17

How to confirm structure of propane by NMR?

2 2 5k
answers votes views
I will really need your help. I am chemist working in the oil buisness and I am interesting is it possible to analyze pr...
ron daedalus 11 Apr 21 '10 at 09:18

How to optimally choose a 1/4J 1H-15N delay for INEPT?

2 1 7k
answers votes views
Why is it often the case that when transferring magnetization from 1H to 15N, the 1/4J time is often a little less than ...
Evgeny Fadeev 5771 Apr 14 '10 at 16:33

How to set up EPR measurement at elevated temperatures?

0 0 3k
answers votes views
What setup do you use to measure EPR at temperatures above room temperature? We have a Bruker EMX500 instrument and we...
Evgeny Fadeev 5771 Apr 14 '10 at 16:28

Why are my acetic acid-d4 solvent peaks off from the expected ppm value?

1 1 8k
answers votes views
Hello there. After running an 1H-NMR experiment I observed the acetic acid-d4 solvent peaks at 11.54 and 21.16 ppm (off...
Evgeny Fadeev 5771 Apr 12 '10 at 15:08

How do you calculate the % or degree of acrylation of a polymer using integrated NMR peaks?

2 1 20452
answers votes views
Hello, I'm trying to use an NMR spectrum to define/calculate a "degree of acrylation" for a PLA-PEG-PLA block copolymer ...
juxtabo 11 Apr 11 '10 at 10:48

In ModelFree calculations how to deal with spins not assigned to models and vice versa?

0 1 5k
answers votes views
What does it mean when modelfree does not assign any model to a particular spin? Also, what should one do if more than h...
Evgeny Fadeev 5771 Apr 07 '10 at 09:13

How to determine the conformation of cis-cyclohexyl derivative by NMR?

1 1 4k
answers votes views
This cis-cyclohexyl derivative with two big substitutes (A and B) may has two conformational isomers, 1 and 2. How to ...
Evgeny Fadeev 5771 Apr 05 '10 at 12:36

How to set up Gaussian pulse to satisfy desired bandwidth?

1 1 11531
answers votes views
Hello, posting this on behalf of my friend. The goal is to set up a gaussian shaped pulse so that bandwidth is X Hertz...
Evgeny Fadeev 5771 Apr 02 '10 at 13:15
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