| 3 |
0 |
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I need help with parameters on a Varian system for Pt-195 NMR. I am having trouble with signal to noise. From what I've ...
| 3 |
0 |
3k |
| answers |
votes |
views |
Does anyone know of a convenient way to automatically save data in VNMR6.1? Occasionally, if an experiment is left to ru...
| 3 |
1 |
6k |
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Hello to all,
This time I am having problem with doing a double resonance experiment. The final goal is to do 1H/19F-HO...
| 3 |
0 |
12343 |
| answers |
votes |
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This is my first time in doing DOSY experiment. i got the data but dont know how to process it.
...
| 3 |
1 |
7k |
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votes |
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I've received a loaner probe from Bruker while ours is being repaired but I'm not getting any timely response on instruc...
| 3 |
0 |
14165 |
| answers |
votes |
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Hi all,
I have a small question on excitation bandwidth for shaped pulses. In many of the literature, the field strength...
| 3 |
0 |
10857 |
| answers |
votes |
views |
Most 90 degree pulse calibration instructions I've run across seem to be for a 1H 90. What about a 13C 90 degree pulse?...
| 3 |
0 |
7k |
| answers |
votes |
views |
Hi All,
I'm new to protein backbone assignment by NMR, and my protein is about ~37kDa (about 400 residues). We've acqui...
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3k |
| answers |
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Hi
I have alraedy seen such a thing, but a google search
now ended up with nothing. Does sbdy now where to by
such smal...
Posted:
fid
139
/ Updated:
oxy
31
Jul 12 '12 at 03:52
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I recently calibrated the 90 for 11B on a Agilent 400MR. The 1H 90 was about 6.8us at 59dB... It turns out to be 22.6u...
