Tagged questions

SSNMR 2H wideline probe that can access sample temperatures in the range of 20-150 K?

1 0 3k
answers votes views
Is anyone aware of NMR facilites, which possess a SSNMR equipped with a 2H wideline probe that can access sample tempera...
Alexey Potapov 21 Jul 04 '11 at 10:24

about sideband in solid-state NMR

2 1 10758
answers votes views
Hi, dear all, I've encounter a strange phenomemon. While the target speed of MAS was set to be 12kHz, the sidebands of ...
Alexey Potapov 21 Jul 04 '11 at 10:17

How to study polymer degradation by gamma and X-Ray radiation?

0 1 3k
answers votes views
Hi, I was asked to study polyethylene degradated by gamma and Xrays. I planed to measure relaxations rates, but which on...
Evgeny Fadeev 5771 Mar 16 '11 at 08:10

optimising o1 in solid state nmr

1 0 4k
answers votes views
I'm a little bit confused about setting o1, in the case of a solid sample First o1 is the offset of the transmitter fre...
silvernmr 11 Mar 09 '11 at 06:17

setting up solid echo on bruker

4 1 8k
answers votes views
Hello, I need to set up aquisition parameters for an echo solid sequence on bruker. In order to analyse deuteraed sample...
silvernmr 11 Mar 06 '11 at 12:39

Inverted Spinning Sidebands

2 0 5k
answers votes views
Hello, My 1H MAS NMR spectrum comes out with the right spinning side band pointing up and the left one pointing down. ...
NMRUser61581 13 Jan 03 '11 at 10:04

How to run 2D ROCSA spectrum only with imaginary on Varian?

2 1 3k
answers votes views
Hi this is Veera Mohan, I have a doubt about setting an experiment, that is I need to run ROCSA solid state nmr experim...
MOHAN 11 Sep 01 '10 at 18:51

How to reference indirect dimensions in Topspin?

0 1 4k
answers votes views
Hello, When I process 3d data on topspin with the ft3d command, I get the three-dimensional spectra, but the chemical sh...
Evgeny Fadeev 5771 Jul 26 '10 at 09:24

14N solid state NMR

4 1 5k
answers votes views
I would like to run some solid state 14N NMR spectra, but I have never run experiment on integer spins in the solid stat...
Joseph DiVerdi 146 May 31 '10 at 06:29

Can adamantane condense in a rotor of a solids probe?

1 0 3k
answers votes views
Hi, does anyone ever get adamantane from the rotor sublimate and condense outside it? A student here found a suspiciou...
Joseph DiVerdi 146 May 31 '10 at 06:25
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