How to start experiment at particular row

i like this post (click again to cancel)

i dont like this post (click again to cancel)

remove favorite mark from this question (click again to restore mark)

I was running a 3D 15N edit NOESY (on a Bruker 600) and it was inadvertently stopped. I would like to restart the experiment starting with the last row that was collected. Does anyone know the command to do this? Any help would be greatly appreciated.

asked Jun 06 '13 at 08:11

Lola Brown
1

One Answer:

oldest newest most voted

i like this answer (click again to cancel)

i dont like this answer (click again to cancel)

Hi Lola,

In principle the "go" command should restart a 2D experiment from where it was stopped. However: this will only work correctly if the pulse program uses the "mc" syntax, rather than "wr #0", and any incrementation/decrementation of pulses, phases or delays must happen within the mc command.

This will be true of the majority of Bruker release sequences, certainly for example noesyhsqcf3gpsi3d - are you using a Bruker standard sequence or something someone else has written?

Before trying this, I would definitely make a copy of the raw data, because I can't guarantee it will work for all software/hardware versions! (seems to work in topspin 3.2, on AVIIIHD).

Pete

link

answered Jun 13 '13 at 11:05

Pete Gierth
401

Here (once you log in) you will be able to sign up for the periodic email updates about this question.

Your answer

Please start posting your answer anonymously - your answer will be saved within the current session and published after you log in or create a new account. Please try to give a good answer, for discussions, please use comments and please do remember to vote (login to vote)

toggle preview

Tags:

bruker ×75
noesy ×26
multizg ×6
command ×1

Asked: Jun 06 '13 at 08:11

Seen: 3,688 times

Last updated: Jun 13 '13 at 11:05

Related questions