Tagged questions

How does removal and re-installation of probe affect shims?

2 0 202
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If you remove and later (not too much later) reinstall the probe and you are confident that probe position inside the ma...
Posted: Evgeny Fadeev 2831 / Updated: Hamish Grant 11 Aug 24 at 17:56

How to remove baseline DC offset in Bruker EMX EPR spectra?

1 0 284
answers votes views
Hello, I've noticed recently that our EPR spectrometer (Bruker EMX500) has a negative offset on the baseline and it bec...
Posted: Evgeny Fadeev 2831 / Updated: Alex Blumenfeld 11 May 12 at 11:55

How to determine physical orientation of X and Y shims?

1 0 280
answers votes views
Hello, I need to help solids lab at our UCI site - they have a custom probe and need to orient it properly in order to e...
Posted: Evgeny Fadeev 2831 / Updated: Carl Gregory 36 Apr 29 at 09:12

Please suggest experiments that push the power limits of NMR probes

2 0 625
answers votes views
I'm trying to come up with reasonable tests of probe performance for all channels by simulating conditions at which arci...
Posted: Evgeny Fadeev 2831 / Updated: Kirk Marat 351 Jan 31 at 14:05

Using probe that started losing B1 strength or has longer 90 degree pulse

1 0 426
answers votes views
I've found that one of our probes lost ~1.5-2 dB of power on 13C, but nutation curve looks OK. There are no random spike...
Posted: Evgeny Fadeev 2831 / Updated: Joseph DiVerdi 136 Apr 19 at 18:07

What may cause lock level depend on pfgon setting in vnmr?

1 0 367
answers votes views
Hello, I've been working through the probe performance tests and noticed that when I change pfgon='yyy' to pfgon='nyn' l...
Posted: Evgeny Fadeev 2831 / Updated: Kirk Marat 351 Jan 15 at 11:47

How to use network analyzer or oscilloscope to tune and match NMR probe?

1 0 711
answers votes views
Hello, could someone share directions on how to tune and match NMR probe RF circuit using a network analyzer? We have a ...
Posted: Evgeny Fadeev 2831 / Updated: Kirk Marat 351 Jan 14 at 11:51

What happens if NMR probe is not perfectly tuned/matched?

2 1 752
answers votes views
What may happen if probe tuning/matching is not perfect besides loss in the sensitivity, any more subtle details? Whoul...
Posted: Magnethead 42 / Updated: carl carter 21 Feb 22 at 16:10

How to set up EPR measurement at elevated temperatures?

0 0 713
answers votes views
What setup do you use to measure EPR at temperatures above room temperature? We have a Bruker EMX500 instrument and we...
Updated: Evgeny Fadeev 2831 Apr 14 at 16:28

How to set up 15N direct detection on UnityInova?

3 0 1k
answers votes views
Has anyone recorded directly detected 15N spectra on UnityInova? We have a triple resonance HCN probe. The sample I've u...
Posted: Evgeny Fadeev 2831 / Updated: Andrew Fowler 51 Jul 30 at 06:01
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