Unanswered questions

NMR transmission, polarized magnetic field and rotation along x' and y' axis

1 0 7k
answers votes views
I am trying to understand the workings of the NMR transmission more closely. I understand how the sinusoidally varying m...
Updated: Aniket 1 May 22 '12 at 10:35

edasp window for 1H/19F double resonance experiment

3 1 6k
answers votes views
Hello to all, This time I am having problem with doing a double resonance experiment. The final goal is to do 1H/19F-HO...
Posted: Amin os 43 / Updated: Kirk Marat 711 Jun 07 '12 at 13:54

Pt 195 NMR Signal to Noise

3 0 5k
answers votes views
I need help with parameters on a Varian system for Pt-195 NMR. I am having trouble with signal to noise. From what I've ...
Posted: Chemist30# 1 / Updated: jkurutz 131 May 21 '12 at 07:59

Sample data request: Bruker HNCO

1 0 4k
answers votes views
Would anyone have a recent generation Bruker HNCO (or similar) data set that they would be willing to share with me for ...
Posted: Kirk Marat 711 / Updated: Jana 31 Jun 20 '12 at 20:02

Why Wobb for 19F is so much dependant on the kind of sample while 1H not?!!

2 0 5k
answers votes views
Normally for 1H, it doesn't matter so much to tune the probe with or without a sample inside. And during the measurement...
Updated: Amin os 43 Jun 06 '12 at 07:26

spinning heating sample in MAS

3 0 3k
answers votes views
there are two known mechanisms: friction heating( which may cause several degrees temperature increase) and induced AC c...
Posted: Jeffreyyyy 1 / Updated: Thiazole 11 Dec 16 '14 at 13:15

Temperature dependence of chemical shift in sodium fluoride aqueous solution.

0 0 2k
answers votes views
I know water is about -0.01ppm/K. How about Na and F? ...
Posted: Jeffreyyyy 1 Apr 29 '12 at 04:03

NMR integral of Hydrophobically modified polyelectrolyte

0 0 3k
answers votes views
Hi there, I have a polyelectrolyte polyethylenimine (PEI) grafted with DSPE-PEG (lipid-polyethylene glycol). I have some...
Posted: leosiu 1 Apr 24 '12 at 13:13

read external file felix

0 0 2k
answers votes views
Hey Everyone, I'm using felix 2007 to analyze my data, and I wonder if it is possible to read external text files. Basic...
Posted: LucaC 1 Apr 13 '12 at 12:38

AMMRL meeting at ENC 2012

1 1 4k
answers votes views
Hello- Is there interest in posting information from the AMMRL meeting at this year's ENC on NMR Wiki? Maybe tweets or ...
Posted: Marc ter Horst 11 / Updated: Jerry Hirschinger 199 Apr 12 '12 at 13:15

set up aromatics experiment in VNMRJ2.2

2 1 3k
answers votes views
Dear Sir, I am new to set up of aromatic assignment experiment. Can you please specify what parameters in VNMRJ 2.2 a...
Updated: Arun Gupta 11 Apr 05 '12 at 22:42

simpson and spinevolution

1 1 4k
answers votes views
Hi, I'm about to start to implement a front end to simpson, and perhaps spinevolution. I wonder if anyone here have some...
Posted: Dune Scientific 11 / Updated: Frey 61 Jun 06 '12 at 19:18

WALTZ-16 decoupling sequence

0 0 3k
answers votes views
Dear all, I am interested in the calculation of WALTZ-16's phase,ie,where comes 0-180-0-...-180-0-180. In addition, the...
Posted: jinghere 11 Mar 28 '12 at 22:31

2D Peak-Picking in Matlab?

1 1 6k
answers votes views
I've got some (phased) 2D spectra and I'd like to create an automated workflow to get a listing of the peak positions, i...
Posted: WaffleWaffle 11 / Updated: Amin os 43 Apr 13 '12 at 05:00

what do you mean by radiation damping give the elementary theory of dispersion. [closed]

0 0 3k
answers votes views
please give me answer on this email id ptsttripathi@gmail.com ...
Posted: praveen tripathi 3 / Updated: Evgeny Fadeev 5771 Mar 27 '12 at 04:18

Macro for variable temperature experiments on Topspin (Bruker)

3 0 10357
answers votes views
I am working on a MAS solid-state NMR Bruker spectrometer using Topspin. Is anyone familiar with a macro for running sev...
Posted: Gili Abr 1 / Updated: David O'Brien 1 Apr 25 '12 at 08:32

VNMRJ 2.2D Macro help

0 0 2k
answers votes views
I am hoping to get some help for setting up a macro to get the NMR to find z0 and auto-shim onto a standard sample after...
Posted: PacmanDave 1 / Updated: Kirk Marat 711 Mar 22 '12 at 06:50

protein-protein complex structure determination

1 0 3k
answers votes views
Dear Friends, I am working on a protein-protein complex using 700MHz VARIAN NMR . I have done HSQC perturbation studi...
Posted: Arun Gupta 11 / Updated: service email start 11 Mar 15 '12 at 17:40

spinner problem [Varian]

3 0 8k
answers votes views
Dear Colleagues, my NMR system recently suffers from problems with spinning the sample. Namely, it does not regulate at...
Posted: d.kubicki 1 / Updated: Jerry Hirschinger 199 Mar 22 '12 at 10:48

How to perform non-selective spectroscopy with an imager?

0 0 2k
answers votes views
Greetings NMR Wiki, I am using a Bruker Biospec 24/30, (100 MHz 1H, DBX, Pv3, XWIN), equiped with a 36mm litz coil prob...
Updated: w101bdk 7 Mar 14 '12 at 10:25

PC rebooted suddenly and Topspin got problem. Has this happened to you?

2 0 4k
answers votes views
Hello all, I was measuring on a Topspin 300MHz and multizg was running (T1ir and cpmg). I unplugged my usb flash memory ...
Updated: Amin os 43 Mar 14 '12 at 02:30

bsms hard ware test on nmr specrometer

1 0 9k
answers votes views
HI nmr wikier I want to test bruker nmr spectometer bsms unit on board level including all boards. How to run the test f...
Posted: JawaidIqbal 1 / Updated: Ulrich Haunz 210 Mar 13 '12 at 04:46

3d Tocsy-hsqc mgnetization transfer problem

1 0 3k
answers votes views
Dear All, I acquired a 3d tocsy-hsqc edited on Bruker machine of small protein in micelles with a mixing time of 70ms. T...
Posted: Mario Scrima 1 / Updated: Mark Girvin 11 Mar 09 '12 at 07:39

1H t2 measurement in solid state nmr

1 0 5k
answers votes views
How to measure t2 of 1H in solid state nmr? we use saturation burst followed by cp to measure T1 of 1H in solid state in...
Posted: vgk 1 / Updated: Ulrich Haunz 210 Mar 05 '12 at 03:34

"quiet" NOESY

1 0 4k
answers votes views
How to set "quiet" NOESY experiment on spectrometer Bruker ? ...
Posted: ilya khodov 1 / Updated: David O'Brien 1 Apr 25 '12 at 08:38

High Pressure NMR Samples

3 0 6k
answers votes views
I need to run NMR on samples of anhydrous ammonia. The boiling point of anhydrous ammonia is -33.34 deg C. In order to...
Posted: grant 1 / Updated: Damodaran Krishnan Achary 21 Feb 28 '12 at 14:09

N15 NNH separated NOESY

2 0 4k
answers votes views
Dear friends, I came across one reference which describe N15 NNH separated NOESY experiment but I am not able to get ...
Posted: Arun Gupta 11 / Updated: Justin Frank 1 Jun 27 '16 at 22:53

HSQC perturbation

0 0 4k
answers votes views
Dear All, I am trying to determine the interaction between 2 proteins. Is there any reference or literature which repo...
Posted: Arun Gupta 11 Feb 13 '12 at 07:04

Isotope Filtered NOESY

1 0 7k
answers votes views
I'm an NMR newbie. I know isotope filtering can be used to study a complex under slow exchange, but for fast-exchange, i...
Posted: Student Tim 1 / Updated: Eugene DeRose 41 Feb 28 '12 at 12:56

incorporating fluorine into proteins

2 0 4k
answers votes views
Hi I was considering the possibility of trying some fluorine NMR and was wanting to know if anyone knew any simple ways...
Posted: Thomas Garner 81 / Updated: sdc 1 Nov 13 '15 at 13:33
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