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Low resolution of pepitde samples

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Dear friends, I am now trying to record the NOESY spectrum of my 30 amino acids peptide on DRX600 with a TXI cryo probe...
Posted: Yun Wang 1 / Updated: Evgeny Fadeev 5771 Jun 07 '11 at 14:00

How do you port pulse sequences to different field strength?

2 0 16741
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Hi, when you set up a pulse sequence at a different magnet field strength - starting with an existing set of parameters ...
Posted: Evgeny Fadeev 5771 / Updated: Kirk Marat 711 Aug 07 '10 at 09:07

How do you port pulse sequences to different field strength?

2 0 16741
answers votes views
Hi, when you set up a pulse sequence at a different magnet field strength - starting with an existing set of parameters ...
Posted: Evgeny Fadeev 5771 / Updated: Kirk Marat 711 Aug 07 '10 at 09:07

How to set NOESY mixing time in intermediate tumbling regime

1 0 8k
answers votes views
I need to run noesy for a monomeric peptide of about 1.5kDa at 800 MHz 1H frequency. NOE peaks are weak at 100 ms mixing...
Posted: Evgeny Fadeev 5771 / Updated: sekhar Talluri 621 Feb 13 '10 at 12:00

Select a reasonable NOESY mixing time given MW, B, viscosity?

2 1 9k
answers votes views
Is there a formula that would suggest a reasonable starting value for the mixing time based on the molecular weight, mag...
Updated: Evgeny Fadeev 5771 Feb 12 '10 at 12:32

Select a reasonable NOESY mixing time given MW, B, viscosity?

2 1 9k
answers votes views
Is there a formula that would suggest a reasonable starting value for the mixing time based on the molecular weight, mag...
Updated: Evgeny Fadeev 5771 Feb 12 '10 at 12:32
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