| 3  | 
                    0  | 
                    21987  | 
                
  
                
                    | answers | 
                    votes | 
                    views | 
                
 
            
         
        
        
            I keep getting myself lost when thinking about saturation pulses, a pulse in which there is no magnetisation in the z di...                
        
        
        
        
        
        
        
        
        
     
    
    
        
        
            
                
                    | 2  | 
                    1  | 
                    6k  | 
                
  
                
                    | answers | 
                    votes | 
                    views | 
                
 
            
         
        
        
            So it is pretty much always recommended to calibrate the 90 for 1H for any 2D experiment... Cosy, Noesy, HSQC, etc...  
...                
        
        
        
        
        
        
        
        
        
     
    
    
        
        
            
                
                    | 1  | 
                    0  | 
                    5k  | 
                
  
                
                    | answers | 
                    votes | 
                    views | 
                
 
            
         
        
        
            Recently while getting a loaner probe up and running, I noticed that the engineers simply had me set the decouple 90 to ...