Can anybody provide parameter file for running 1 D STD saturation transfer difference experiment with DPFGSE sculpted solvent suppresion on varian 600 MHz instrument. asked Sep 23 '09 at 06:49 sns03003 |
looks like there is macro satxfer_dpfgse if you call it, most parameters will be set correctly. I've set up a simple manual page, which lists the adjustible parameters for this sequence. Also, if you are curious you can read the text of the pulse sequence: type
in the UNIX command line (assuming that your system files are in /vnmr directory). There are three literature references that describe details of the sequence. Probably the less usual part of the sequence is that it uses fine power control for the solvent-selective 180 pulse (associated with parameters To start with - set answered Sep 28 '09 at 12:07 Evgeny Fadeev |