NH---O hydrgen bond detection in N-(2-methoxyphenyl)benzamide

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I'd like to know if there are further NMR spectroscopic methods to detect NH---O hydrogen bond in N-(2-methoxyphenyl)benzamide compounds. I know about HNCO techniques, but they are specifc for carbonyl carbon. I have already tried to reveal any amide proton chemical shift variation with temperature and to measure the 1JNH by 1H,15N HSQC spectra, but I don't think these observables could be sufficient to show any scalar coupling between the methoxy oxygen and the amide proton.

hydrogen-bond

asked Oct 19 '14 at 12:48

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0	Here is a topic concerning similar issue: http://qa.nmrwiki.org/question/79/what-nmr-experiments-can-be-used-to-detect-hydrogen-bonds link answered Oct 24 '14 at 00:48 Arkadiusz Leniak 238

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Asked: Oct 19 '14 at 12:48

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Last updated: Oct 24 '14 at 00:48

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