Unanswered questions

Help for Boron 11 NMR!

10 1 16230
answers votes views
I'm using a Bruker 300 NMR, equipped with a BBO probe, to do Boron 11 NMR. But I got no signal no matter what pulse leng...
Jim Lin 1 Apr 14 '15 at 06:47

Bruker AV500 TOPSHIM error

1 0 4k
answers votes views
Hi, I'm having a problem with topshim on Bruker AV 500 using topspin 2.1. it finishes with error (topshim: FieldMap - no...
Jim Lin 1 Apr 14 '15 at 06:23

nmr phenylethylamine

2 0 3k
answers votes views
hello...i know only the basics on nmr and need some help :i need H-NMR help with phenylethylamine Phe-CH2-CH2-NH-R - how...
Jim Lin 1 Apr 09 '15 at 07:59

31P-31P COSY

1 0 4k
answers votes views
I like to run a 31P-31P COSY experiment to determine whether there is coupling between 1R-31P-CH2-31P-X in my molecule. ...
Jim Lin 1 Apr 09 '15 at 07:54

Topshim error

2 0 8k
answers votes views
HELLO all nmr wikier,I am facing problem in runing topshim on bruker 500Mhz using topspin 2.1 it finishes with error (fi...
Jim Lin 1 Mar 31 '15 at 06:19

distorted DOSY ID

9 1 8k
answers votes views
Why are some Dosy spectra 1d so distorted (like the one below)?. How can this be overcome? ...
Umayal Rakesh 1 Mar 30 '15 at 00:08

Absence of some signals on 1H and 13C spectra of polyaromatic carboximidate

3 0 7k
answers votes views
Hi, I have encountered a strange behaviour of some signals (they are absent) in a series of polycyclic aromatic carboxi...
zablociak 21 Mar 23 '15 at 12:11

splitting QCPMG echo train

0 0 1k
answers votes views
Hi all, I'm running qcpmg (qcpmgaq), using bruker topspin3. Does anyone have a suggestion how to split the echos train? ...
shon roni 1 Mar 23 '15 at 04:07

How to calcualte eoors in ppm from Hz of Hsqc data?

1 0 3k
answers votes views
Hi all, I want to calculate error in ppm from my Hsqc data. My spectrometer yields X1axis, Y1Axis, DX1, DY1, X1ppm, and ...
Arkadiusz Leniak 238 Mar 17 '15 at 02:10

Why NMR can deliver angstrom reolution structures.

1 0 2k
answers votes views
How can NMR operating at radiofrequency wavelengths deliver angstrom resolution? For example X-ray crystallography opera...
Arkadiusz Leniak 238 Mar 17 '15 at 01:10
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