I am facing problems in calibration of my HCCH-TOCSY spectrum in reference to HBHACONH and HCCCONH spectrum. Can somebody tell me how to solve this issue? Can I autoassign my HCCH-TOCSY spectrum using HBHACONH spectrum asked Oct 01 '11 at 21:55 Arun Gupta |
If you talk about hcchdigp3d : HCCH-TOCSY spectrum are shift by SW/4 in proton indirect dimension if you don't correct it. Read in pulseprog file, near the end, there are some indications about processing to correct this shift : ;Processing ;SR(F1): 1/4 SWH(F1) So process your data without take care about calibration and after shift proton indirect dimension of SW/4 in your spectrum viewer. hope that can help you and guess I've really understood the question. answered Oct 02 '11 at 08:08 Yoan Monneau |