The procedures that you want will be found in Bruker's manual: "Acceptance Test Procedures for Avance NMR Systems". There should be a copy with your system. After you have calibrated the hard pulses, you need to fill them into the "prosol" table. The You will normally only have to do the hard pulse calibration procedures, as the prosol editor will generally calculate all of the low level (decoupler) and shaped pulses for you.