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posted Aug 26 '09 at 14:41

Scott%20Robson's gravatar image

Scott Robson
156

1/4J 1H-15N delay times

Why is it often the case that when transferring magentization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

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No.1 Revision

posted Aug 26 '09 at 15:25

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

1/4J 1H-15N delay times

Why is it often the case that when transferring magentization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

click to hide/show revision 3
No.2 Revision

posted Aug 26 '09 at 15:45

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

1/4J 1H-15N delay times

Why is it often the case that when transferring magentization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

click to hide/show revision 4
No.3 Revision

posted Aug 27 '09 at 00:13

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

Optimal choice of 1/4J 1H-15N delay timestimes in INEPT

Why is it often the case that when transferring magentization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

click to hide/show revision 5
No.4 Revision

posted Aug 27 '09 at 00:19

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

Optimal choice of 1/4J 1H-15N delay times in INEPT

Why is it often the case that when transferring magentization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

click to hide/show revision 6
No.5 Revision

posted Nov 18 '09 at 14:26

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

Optimal choice of 1/4J 1H-15N delay in INEPT

Why is it often the case that when transferring magentization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

click to hide/show revision 7
bumped question to the top of the list

posted Jan 22 '10 at 12:23

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

Optimal choice of 1/4J 1H-15N delay in INEPT

Why is it often the case that when transferring magentization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

click to hide/show revision 8
fixed typo

posted Jan 22 '10 at 12:24

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

Optimal choice of 1/4J 1H-15N delay in INEPT

Why is it often the case that when transferring magentization magnetization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

click to hide/show revision 9
No.8 Revision

posted Apr 14 '10 at 16:33

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

Optimal choice of How to optimally choose a 1/4J 1H-15N delay in INEPTfor INEPT?

Why is it often the case that when transferring magnetization from 1H to 15N, the 1/4J time is often a little less than expected - for example, it is often set to 2.25 ms. On the other hand, when transferring back form 15N to 1H for detection, 1/4J is typically set accurately to 2.7 ms?

I'm assuming the answer is something to do with relaxation of 1H during INEPT transfer. How necessary is this? Is there a way to optimize the values based on t2 time rather than sit at the magnet and manually optimize them?

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