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posted Jun 02 '14 at 09:26

Arkadiusz%20Leniak's gravatar image

Arkadiusz Leniak
238

19F full range homodecoupling

Greetings, this is my first question in this wiki :)

I wonder if there's possibility to obtain full homo decoupled spectrum of 19F. Spectrum of my compound is quite complicated becouse of 19F-19F couplings. I have BBOF probe for Bruker Avance III HD spectrometer. 19F is tuned at broadband coil. If there's any possibility to make that, please give me some clues. Thanks, Arek

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posted Jun 02 '14 at 09:46

Arkadiusz%20Leniak's gravatar image

Arkadiusz Leniak
238

19F full range homodecoupling

Greetings, this is my first question in this wiki :)

I wonder if there's possibility to obtain full homo decoupled spectrum of 19F. Spectrum of my compound is quite complicated becouse of 19F-19F couplings. I have BBOF probe for Bruker Avance III HD spectrometer. 19F is tuned at broadband coil. If there's any possibility to make that, please give me some clues. Thanks, Arek

EDIT I have obtained projection that looks like the one I need. Projection from 2D 19F J-res spectrum. I wonder if there's some kind of pureshift experiments designated for fluorine

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