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posted Apr 29 '12 at 10:39

Jeffreyyyy's gravatar image

Jeffreyyyy
1

spinning heating sample in MAS

there are two known mechanisms: friction heating( which may cause several degrees temperature increase) and induced AC current heating( in this paper:Electrical and ionic conductivity effects on magic-angle spinning nuclear magnetic resonance parameters of CuI. which can heat sample over 100 Celsius.) My question is, has any body seen this heating in MAS NMR?

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posted Apr 29 '12 at 10:39

Jeffreyyyy's gravatar image

Jeffreyyyy
1

spinning heating sample in MAS

there are two known mechanisms: friction heating( which may cause several degrees temperature increase) and induced AC current heating( in this paper:Electrical and ionic conductivity effects on magic-angle spinning nuclear magnetic resonance parameters of CuI. which can heat sample over 100 Celsius.) My question is, has any body seen this heating in MAS NMR?

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