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initial version
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Dear NMR wikiers
iam assigning 95 aminoacid residue protein . i can see 76 cross peaks in hsqc on 700 vnmr cryob . still some peaks are missing . i tried at modified ph conditions , buffer ionic strength and d2o percentage ( 5 to 10 percent ).but no significant improvement
is their any experment to get best number of cross peaks ?
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No.1 Revision
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Dear NMR wikiers
iam assigning 95 aminoacid residue protein . i can see 76 cross peaks in hsqc on 700 vnmr cryob . still some peaks are missing . i tried at modified ph conditions , buffer ionic strength and d2o percentage ( 5 to 10 percent ).but no significant improvement
is their any experment to get best number of cross peaks in hsqc ?
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3 |
No.2 Revision
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Dear NMR wikiers
iam I am assigning 95 aminoacid residue protein . i I can see 76 cross peaks in hsqc N H HSQC on 700 vnmr cryob . still some peaks are missing .
i I tried at modified ph conditions , buffer ionic strength and d2o percentage ( 5 to 10 percent ).but no significant improvement
is their any experment to get best number of cross peaks in hsqc ?
