Hello,
I am running 1H MAS NMR on a hydroxylated metal oxide material. I use 3us pulse width, 5 sec acquisition time, and my sweep width is 100kHz. Also, I am using a 600 MHz Varian magnet, 5mm rotor, and spinning at 10kHz.
My spectrum comes out with the right spinning side band pointing up and the left one pointing down. What does that mean?
Thank you very much