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posted Apr 02 '14 at 23:19

SankarampadiAravamudhan's gravatar image

SankarampadiAravamudhan
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We just bought a new console (with Topspin 3.2)for our Bruker 400 and noticed that not all experiments that we previously used to run are setup on the new version. For instance, 195Pt experiment is not working. The message that appeared when we tried it was: "Cannot perform getprosol. The following files are not found. Observe pulses for 195Pt. DE and Trim pulses for 195Pt". Could any one help with the step-by-step procedure for setting up this experiment? Perhaps the probe file is not populated with pulses for 195Pt. We would greatly appreciate your help. It may probably be appropriate to answer this question by narrating a similar instance, and I recall such an instance of about 20 years before:- an experience with AC300 Bruker NMR Spectrometer which was in use at that time in North Eastern Hill University, Shillong, INDIA. I was trying to implement a J-Scaling pulse sequence, from the Library of Automation Programs (set of Bruker .AU extension files provided in a Diskette). When the Program was set up and the Command was given to run, the monitor returned a prompt as if nothing has happened. No error Messages, nor any other consequence of trying to run the instruction set. (In the case of this query on 195pt, an error message seems to result). For the case of J-scaling with AC300, I sent a message to the Bruker India Scientific, and after a while I was informed that these pulse programs in the Diskette where not tried out and run in the AC300 spectrometer housed at North Eastern Hill University. Such case histories prompt me to suggest that it would be better to contact the supplier, rather than any other user of similar packages. I am not sure whether, queries in nmrwiki get answered by the Bruker Engineers. S.Aravamudhan
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posted Apr 02 '14 at 23:20

SankarampadiAravamudhan's gravatar image

SankarampadiAravamudhan
91

We just bought a new console (with Topspin 3.2)for our Bruker 400 and noticed that not all experiments that we previously used to run are setup on the new version. For instance, 195Pt experiment is not working. The message that appeared when we tried it was: "Cannot perform getprosol. The following files are not found. Observe pulses for 195Pt. DE and Trim pulses for 195Pt". Could any one help with the step-by-step procedure for setting up this experiment? Perhaps the probe file is not populated with pulses for 195Pt. We would greatly appreciate your help.

It may probably be appropriate to answer this question by narrating a similar instance, and I recall such an instance of about 20 years before:- an experience with AC300 Bruker NMR Spectrometer which was in use at that time in North Eastern Hill University, Shillong, INDIA.

I was trying to implement a J-Scaling pulse sequence, from the Library of Automation Programs (set of Bruker .AU extension files provided in a Diskette). When the Program was set up and the Command was given to run, the monitor returned a prompt as if nothing has happened. No error Messages, nor any other consequence of trying to run the instruction set. (In the case of this query on 195pt, an error message seems to result). For the case of J-scaling with AC300, I sent a message to the Bruker India Scientific, and after a while I was informed that these pulse programs in the Diskette where not tried out and run in the AC300 spectrometer housed at North Eastern Hill University. Such case histories prompt me to suggest that it would be better to contact the supplier, rather than any other user of similar packages. I am not sure whether, queries in nmrwiki get answered by the Bruker Engineers. S.Aravamudhan

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