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posted Mar 20 '14 at 10:04

Kirk%20Marat's gravatar image

Kirk Marat
711

Yes, your prosol file is not set up correctly. You can avoid using the getprosol command in the "new" dialog by unchecking the appropriate box. You then have to set the pulse lengths and power levels manually. Once you have the 90 degree pulses calibrated enter them into "edprosol" (see manual), and "edprosol" will calculate any other pulses. You will also need to enter a value for DE (6.5 to 8 usec is typical) and trim pulses (2.5 ms is typical). It is recommended that you use "getprosol" for setting the pulses and powers. If you have "powcheck" enabled (recommended) you may need to enter a power limit into probe file. If you are not sure of what power level is safe, please consult Bruker
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No.1 Revision

posted Mar 20 '14 at 10:06

Kirk%20Marat's gravatar image

Kirk Marat
711

Yes, your prosol file is not set up correctly. You can avoid using the getprosol command in the "new" dialog by unchecking the appropriate box. You then have to set the pulse lengths and power levels manually.

Once you have the 90 degree pulses calibrated enter them into "edprosol" (see manual), and "edprosol" will calculate any other pulses. You will also need to enter a value for DE (6.5 to 8 usec is typical) and trim pulses (2.5 ms is typical).

It is recommended that you use "getprosol" for setting the pulses and powers.

If you have "powcheck" enabled (recommended) you may need to enter a power limit into probe file. If you are not sure of what power level is safe, please consult BrukerBruker, but a power level similar to that for 13C would be reasonable.

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No.2 Revision

posted Mar 20 '14 at 10:10

Kirk%20Marat's gravatar image

Kirk Marat
711

Yes, your prosol file is not set up correctly. You can avoid using the getprosol command in the "new" dialog by unchecking the appropriate box. You then have to set the pulse lengths and power levels manually.

Once you have the 90 degree pulses calibrated calibrated, enter them into "edprosol" (see manual), and "edprosol" will calculate any other pulses. You will also need to enter a value for DE (6.5 to 8 usec is typical) and trim pulses (2.5 ms is typical).

It is recommended that you use "getprosol" for setting the pulses and powers.

If you have "powcheck" enabled (recommended) you may need to enter a power limit into probe file. file ("edhead"). If you are not sure of what power level is safe, please consult Bruker, but a power level similar to that for 13C would be reasonable.

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