Hello,
First you can use the command multi_zgvt. This is an au macro programm from Bruker.
/*
/*** ^^A
--C++-- ***************/ / multizgvt -*-C++-*- **********************************************/ /* multi_zgvt 18.05.2000 */
/************************************************************//****************************************************************/ /* Short Description : */ /* Performs multiple acquisitions on increasing expnos */ /* with temperatures that are read from a vtlist file. *//************************************************************//****************************************************************/ /* Keywords : */ /* serial acquisitions, variable temperature, VT *//************************************************************//****************************************************************/ /* Description/Usage : */ /* This AU program performs multiple acquisitions on */ /* increasing expnos in much the same way as multizg. If */ /* datasets do not yet exist, the current dataset and its */ /* parameters are copied. If the data sets already exist, */ /* then the experiments are executed as they are. */ /* But in addition to multizg, this AU program asks for a */ /* variable temperature list and sets the temperature for */ /* each experiment according to the list entry from the */ /* VTLIST file. */ /* The number of experiments is calculated from the number */ /* of temperature values in the VTLIST. The user can ask */ /* for a reduced number of experiments, though. */ /* A security check is implemented that asks for a */ /* confirmation of the highest and lowest temperature of */ /* the variable temperature list. */ /* Temperatures are in Kelvin K ! */ /* You will be asked for the temperature equilibration */ /* time. The AU program will wait at as long as defined */ /* by this time for the temperature to settle. */ /* The total experiment time is estimated and printed out. *//************************************************************//****************************************************************/ /* Author(s) : */ /* Name : Rainer Kerssebaum, Mike Engelhardt */ /* Organisation : Bruker BioSpin GmbH */ /* Email : rainer.kerssebaum@bruker.de */ /* : michael.engelhardt@bruker.de *//************************************************************//****************************************************************/ /* Name Date Modification: */ /* rke, eng 990711 created */ /* eng 000327 switch ZGSAFETY off if on */ /* eng 000518 bug 2388 corrected */ /* eng 000518 PathSystemTemp instead of /tmp */ /* wem 080905ZGOVERWRITE / /*********************/ZG_OVERWRITE */ /****************************************************************/
This was the header of the macro!
The vt-list you find under AcquPars and Lists. With the ... Button you can choose a saved vt-list. With the E-Button you can edit your own vt-list and save it there.
Second possiblity, you can use IconNMR instead the multi_zgVT makro. Here you can treat numbers of samples of the automation sampler, maybe also of the HR-MAS sampler!?
In the Configuration you have the Temperature Handling. I click on Post Insertion Set/Check and there the "Temperature Setting after Sample Insertion" choose "according to each experiment's TE Parameter". Then you put the TE parameter into the "User Specific Parameters/Commands" in the "User Manager" and then you can change the Temperature easily for every Experiment.
With low temperature I had the problem, that I have to change the gas flow meanwhile I go down in temperature. ...
Kind Regards
Anke