Revision history [back]
click to hide/show revision 1
initial version

posted May 10 '11 at 11:55

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

Try using 15N edited NOESY and TOCSY, these are very complimentary to the triple resonance experiments. Also - in the case you have overlapped peaks - look at them in all three dimensions, that way you can resolve them better. Sparky allows switching the axes on the display plane easily. Command **xr** rotates the spectrum in 3D, also it helps to center view on a peak before rotations - select a peak and then type **vc**.
click to hide/show revision 2
No.1 Revision

posted May 10 '11 at 11:55

Evgeny%20Fadeev's gravatar image

Evgeny Fadeev
5771

Try using 3D 15N edited NOESY and TOCSY, these are very complimentary to the triple resonance experiments.

Also - in the case you have overlapped peaks - look at them in all three dimensions, that way you can resolve them better. Sparky allows switching the axes on the display plane easily. Command xr rotates the spectrum in 3D, also it helps to center view on a peak before rotations - select a peak and then type vc.

powered by CNPROG