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posted Mar 20 '11 at 07:54

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Clemens Anklin
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The ideal experiment for this is the HMBC. The delay should be optimized for ca 5 Hz coupling.
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posted Mar 20 '11 at 16:00

Clemens%20Anklin's gravatar image

Clemens Anklin
416

The ideal experiment for this is the HMBC. The delay should be optimized for ca 5 Hz coupling. The nJ(C,H) couplings across oxygens or other heteroatoms can be smaller than the corresponding ones over all carbons.

You might also be able to establish connectivity with a NOESY or ROESY experiment.

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