Maybe it's just shimming problem, did you try 5 mM tube and spin the sample?sample? Are X and Y shims optimized?
Was your magnet recently energized or shim files are brand new?
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Maybe it's just shimming problem, did you try 5 mM tube and spin the sample?sample? Are X and Y shims optimized?
Was your magnet recently energized or shim files are brand new?