Maybe it's just shimming problem, did you try 5 mM tube and spin the sample?sample? Are X and Y shims optimized?
Was your magnet recently energized or shim files are brand new?
1 |
initial version
|
posted Nov 19 '10 at 12:17 Magnethead |
2 |
No.1 Revision
|
posted Nov 19 '10 at 12:18 Magnethead |
Maybe it's just shimming problem, did you try 5 mM tube and spin the sample?sample? Are X and Y shims optimized?
Was your magnet recently energized or shim files are brand new?