Tagged questions

using chenomx and missing peaks

1 0 3k
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hello, I am trying to identify and quantify of metabolites present in semen with spectra obtained from 400 MHz NMR using...
Posted: Reza mohammadi 1 / Updated: Ulrich Haunz 210 Feb 10 '14 at 01:36

Relative quantification (residual solvents)

2 0 32773
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Hi All, I've been trying to get a clear answer to this question for a while now, but can't seem to get a definitive ...
Posted: organicadam 1 / Updated: John Hollerton 96 Dec 09 '13 at 09:37

Help solving a spectrum!

2 0 3k
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Can someone please help me solve an nmr problem? I've tried a lot but can't get it. Please post ur email and i'll send y...
Posted: Lyra 1 / Updated: vaclavrimal 11 Aug 08 '13 at 04:44

NMR Vs X ray crystal data not matching each other

2 0 3k
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I had a very weird situation where my compound shows double bond between carbons in NMR but shows it as single bond in x...
Posted: shanku 1 / Updated: John Hollerton 96 Dec 09 '13 at 09:57

2-Methoxybenzaldehyde

2 0 5k
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Hey everyone, I've started practicing reading NMR again after having not done so for years, and I'm getting caught up o...
Posted: John Xavier 1 / Updated: Pete Gierth 401 Jun 17 '13 at 12:06

how to simulate the impression of excitation of cpmg

0 0 2k
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Hi? recently I try to use the bloch equation to simulate the magnetization M's variation, i used the perfect 90-degr...
Posted: da hsu 1 Apr 18 '13 at 18:51

Longer pulse length for conducting samples?

3 0 5k
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Hi, my 1H 90 deg pulses are always longer when I work with my samples that are electrically conducting. Is this a/the re...
Posted: Santhosh 1 / Updated: glass lizard 31 Aug 12 '12 at 12:24

33S NMR Experiment

1 1 5k
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Dear Everyone I´d like to run 33S-NMR experiments using a Bruker NMR spectrometer at 400 MHz buy I nedd the pulse seque...
Posted: Juan_Carlos 11 / Updated: Pete Gierth 401 Jun 15 '12 at 07:53

High Pressure NMR Samples

3 0 6k
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I need to run NMR on samples of anhydrous ammonia. The boiling point of anhydrous ammonia is -33.34 deg C. In order to...
Posted: grant 1 / Updated: Damodaran Krishnan Achary 21 Feb 28 '12 at 14:09

Simple 1H-NMR Assignment Query

4 1 5k
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Hi guys, sorry to be really cheeky and sign up simply to ask for help, but here goes. I've done a simple Grignard addit...
Posted: Brianstorm 11 / Updated: 3nath 11 Oct 26 '11 at 12:53
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