Unanswered questions

How to display NMR structure of molecule with non-standard residues?

1 0 10828
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... solving a structure of a cyclic peptide with Ornithine residue, where Orn side-chain participates in an amide bond. ...
Updated: Evgeny Fadeev 5771 Feb 02 '10 at 08:59

Absorption of RF energy quantum and change of the nucleus spin state

1 0 8k
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Is a quantum of energy such as that in transverse RF field produced by NMR probe absorbed instantaneously by a single nu...
Updated: Evgeny Fadeev 5771 Jan 26 '10 at 13:42

NMR experiments to assign aromatic sidechains?

3 1 9k
answers votes views
Hello, may I ask this - NMR experiments/pulse sequences are available to assign aromatic sidechains - Phe, Tyr, Trp? We'...
Posted: anita 31 / Updated: roseyp 46 Feb 22 '11 at 09:38

Example of XPLOR NMR structure with unnatural custom residues

0 2 3k
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Hi there! Could anyone share an example of NIH-XPLOR files for annealing of NMR structure with non-natural residues. May...
Updated: anita 31 Jan 19 '10 at 11:40

What may cause lock level depend on pfgon setting in vnmr?

2 1 5k
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Hello, I've been working through the probe performance tests and noticed that when I change pfgon='yyy' to pfgon='nyn' l...
Posted: Evgeny Fadeev 5771 / Updated: Jerry Hirschinger 199 Sep 28 '10 at 12:12

How to set NOESY mixing time in intermediate tumbling regime

1 0 8k
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I need to run noesy for a monomeric peptide of about 1.5kDa at 800 MHz 1H frequency. NOE peaks are weak at 100 ms mixing...
Posted: Evgeny Fadeev 5771 / Updated: sekhar Talluri 621 Feb 13 '10 at 12:00

How to use network analyzer or oscilloscope to tune and match NMR probe?

1 0 10504
answers votes views
Hello, could someone share directions on how to tune and match NMR probe RF circuit using a network analyzer? We have a ...
Posted: Evgeny Fadeev 5771 / Updated: Kirk Marat 711 Jan 14 '10 at 11:51

How to extract Bruker fid data - in topspin and xwinnmr - to ascii format?

4 1 23838
answers votes views
Hi and thanks for answering my prev. questions! Decided to ask this one: How can I convert fid data (ser file) to plain...
Posted: Magnethead 42 / Updated: Ulrich Haunz 210 Dec 04 '14 at 04:16

1H-NMR-spektrum for CAS: 1792-81-0 HEEEELP

3 1 7k
answers votes views
I'm going to finish my repport for the school in a very few days, but I just can't finde a 1H-NMR-spektra for the molecy...
Posted: say 11 / Updated: Clemens Anklin 416 Dec 23 '09 at 14:58

Helium recovery system

2 1 7k
answers votes views
How do I configure a helium recovery system that won't perturb my magnet's stability? I'm concerned that just hooking ...
Posted: jkurutz 131 / Updated: Jerry Hirschinger 199 Jul 23 '14 at 10:45
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