Bruker phase image recon

0 0 60
answers votes views
Hi all- I'm acquiring 1-2s/dynamic, single-slice gradient echo image series over a period of 10 minutes or so. By defau...
Posted: Nicholas E 11 Apr 17 at 08:35

dept nuclear magnetic resonance

0 0 245
answers votes views
what it the difference between c13 and dept nmr? ...
Posted: dereje sharew 1 Apr 11 at 15:53

Bruker AV500 TOPSHIM error

1 0 73
answers votes views
Hi, I'm having a problem with topshim on Bruker AV 500 using topspin 2.1. it finishes with error (topshim: FieldMap - no...
Posted: jrlopez 1 / Updated: Jim Lin 1 Apr 14 at 06:23

nmr phenylethylamine

2 0 94
answers votes views
hello...i know only the basics on nmr and need some help :i need H-NMR help with phenylethylamine Phe-CH2-CH2-NH-R - how...
Posted: ann choroshun 1 / Updated: Jim Lin 1 Apr 09 at 07:59

Distorted/antiphase signals when doing Dosy

3 0 111
answers votes views
Hello, I am running Dosy experiment using ledbpgp2s sequence. I am getting sort of signal distortions. I tried the solu...
Posted: Umayal Rakesh 1 / Updated: gravatar 71 2 days ago

31P-31P COSY

1 0 246
answers votes views
I like to run a 31P-31P COSY experiment to determine whether there is coupling between 1R-31P-CH2-31P-X in my molecule. ...
Updated: Jim Lin 1 Apr 09 at 07:54

splitting QCPMG echo train

0 0 62
answers votes views
Hi all, I'm running qcpmg (qcpmgaq), using bruker topspin3. Does anyone have a suggestion how to split the echos train? ...
Posted: shon roni 1 Mar 23 at 04:07

How to calcualte eoors in ppm from Hz of Hsqc data?

1 0 128
answers votes views
Hi all, I want to calculate error in ppm from my Hsqc data. My spectrometer yields X1axis, Y1Axis, DX1, DY1, X1ppm, and ...
Posted: ick lad 1 / Updated: Arkadiusz Leniak 213 Mar 17 at 02:10

Why NMR can deliver angstrom reolution structures.

1 0 111
answers votes views
How can NMR operating at radiofrequency wavelengths deliver angstrom resolution? For example X-ray crystallography opera...
Posted: Anon 1 / Updated: Arkadiusz Leniak 213 Mar 17 at 01:10

Absence of some signals on 1H and 13C spectra of polyaromatic carboximidate

3 0 681
answers votes views
Hi, I have encountered a strange behaviour of some signals (they are absent) in a series of polycyclic aromatic carboxi...
Posted: Arkadiusz Leniak 213 / Updated: zablociak 21 Mar 23 at 12:11

reading Bruker phase data

1 0 102
answers votes views
Hi all, I'm having trouble reading the 2dseq file for a scan I ran. It should contain 2 slices of 66x50 voxels, repeate...
Updated: Nicholas E 11 Mar 13 at 10:53

WaterLOGSY pulse program for bruker

1 0 464
answers votes views
Hello, I was wondering if there was a waterLOGSY sequence among the bruker sequences. If not, could someone tell me whe...
Posted: gravatar 71 / Updated: Arkadiusz Leniak 213 Mar 17 at 08:09

OH, NH, SH Labile protons in water nmr

1 0 177
answers votes views
Hello all, Just to mirror Craig Grimmer's question about labile protons in non-aqueous solvents, does anyone know of an...
Posted: gravatar 71 / Updated: Arkadiusz Leniak 213 Mar 14 at 11:24

Mechanism of chemical exchange between labile protons (OH, NH, SH)

1 0 136
answers votes views
Hello All Does anyone know of any good articles dealing with the mechanisms of labile proton exchange in non-aqueous so...
Posted: Craig Grimmer 41 / Updated: gravatar 71 Mar 09 at 02:28

Topshim error

2 0 192
answers votes views
HELLO all nmr wikier,I am facing problem in runing topshim on bruker 500Mhz using topspin 2.1 it finishes with error (fi...
Posted: feroon 21 / Updated: Jim Lin 1 Mar 31 at 06:19

noisy hmqc and hmbc spectra

2 0 207
answers votes views
Hey all! We've got a serious problem because with our new probe (5mm bbo bruker) the t1 noise in the heteronuclear corr...
Posted: apophis 1 / Updated: Pete Gierth 401 Feb 25 at 14:06

Choice of relaxation delay time (d1) in 2D experiments.

1 0 177
answers votes views
Hi, Most people tend to use a lower d1 for 2D than for 1D. Help me understand why. Furthermore, supposing you know you...
Updated: gravatar 71 Mar 09 at 02:21

log: Failed to find Z0 - low s/n

2 0 156
answers votes views
Hi, everybody! I met a problem on Varian 400 MR: DMSO samples don't lock by "find Z0" button, but I can find lock signal...
Posted: Ilya N 1 / Updated: Ulrich Haunz 248 Mar 09 at 09:18

Coherence transfer pathway for Magic sandwich echo

0 0 178
answers votes views
Hi, I am writing the pulse sequence for magic sandwich echo*, but I am stuck with the phase cycle since I don't have a ...
Updated: Traveller 1 Feb 15 at 15:59

Any decent nmr processing software for free?

5 0 279
answers votes views
Hello people, Does anyone know of any free NMR software (no trials, I can't stand it anymore) that is robust enough to ...
Posted: gravatar 71 / Updated: Craig Grimmer 41 Mar 05 at 01:45

Parameters for zgesfpgp 1d experiment (flipback watergate) on Bruker

1 0 347
answers votes views
Hi , Does any one know how to set up the zgesfpgp 1d experiment (flipback water gate) on Bruker. I am looking for p29 du...
Posted: sri 71 / Updated: Clemens Anklin 416 Mar 03 at 20:41

building chains of resonance groups from connectivities

0 0 124
answers votes views
Greetings, Given a dictionary of connectivities of the following form: residue i -> possible residues i-1 : 54 -&g...
Posted: Thomas 1 Feb 07 at 11:36

How do I perform a 2D C-13-C-13 spectrum simulation?

0 0 152
answers votes views
I am new to NMR pipe and was wondering how to perform a carbon-13 carbon-13 simulation in NMR pipe? For example, what th...
Posted: epsaliba 1 Feb 06 at 07:28

Can anyone point me towards a waterlogsy tutorial for bruker?

0 0 184
answers votes views
Hello people, It's all in the title. ...
Posted: gravatar 71 Feb 02 at 08:15

adequate NMR

0 0 143
answers votes views
Hi, I am really confused about reading the adequate 1J(CC) results, Can anyone help me with that? What is the differenc...
Posted: Hessen 1 Jan 29 at 14:57

ADC value, help!!!

1 0 166
answers votes views
ADC value in Bruker 1T, please tell me how to get it? ...
Posted: Huong Nguyen 1 / Updated: Ulrich Haunz 248 Feb 09 at 07:37

Measurement of very short T2

1 0 230
answers votes views
Hello, I'm measuring T2 in paramagnetic materials. These values are very short (0.5-5 ms), and I have to use very short...
Posted: A K 1 / Updated: Jeffreyyyy 1 Feb 27 at 12:48

how many percent peak in NH HSQC enough to solve structure?

1 0 281
answers votes views
Hello everyone, I have a stupid question and often confuse me. We often meet peak missing in 15N H HSQC,but usually ho...
Posted: chengkun wang 1 / Updated: sekhar Talluri 601 Feb 14 at 23:21

Predicting aquisition time needed depending on sample concentration

2 0 4k
answers votes views
Hi , is there a way of predicting aquisition time needed depending on sample concentration in order to get a decent spe...
Updated: gravatar 71 Mar 12 at 09:35

bigger MAS-NMR spectrum as irradiation window

0 0 441
answers votes views
Hi, I have a sample with a very very big CSA which is broader than my irradiation windows, so I have to acquire my dat...
Posted: Thiazole 11 Dec 16 '14 at 13:05
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